反应条件
in tetrahydrofuran THF was distilled onto Te powder under N2, frozen (-196°C), MeLi syriged in, mixt. was allowed to thaw, after Te dissolution mixt. was refrozen (-196°C), Cl(CH2)3Cl added, warmed to room temp.; mixt. was hydrolyzed (satd. aq. NaCl), org. phase septd., dried, evapd. in vacuo;
参考文献
Hope, Eric G.; Kemmitt, Tim; Levason, William
Organometallics, 1987 , vol. 6, p. 206 - 207