(E)-3-(2-硝基苯基)丙-2-烯酸乙酯合成路线 （共 33 条）
反应条件
1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: 2-nitro-benzaldehyde in tetrahydrofuran T=0 - 20°C; 8 h;
参考文献
Ni, Lijun; Li, Ziyuan; Wu, Fan; Xu, Jinyi; Wu, Xiaoming; Kong, Lingyi; Yao, Hequan
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1271 - 1274
反应条件
potassium phosphate; [((ferrocenyl)(C(CH3)N(C6H4)CH3))PdCl(N,N'-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)]; tetrabutylammomium bromide in N,N-dimethyl-formamide T=140°C; Heck reaction; 2 h; Inert atmosphere;
参考文献
Ren, Gerui; Cui, Xiuling; Yang, Erbing; Yang, Fan; Wu, Yangjie
Tetrahedron, 2010 , vol. 66, # 23 p. 4022 - 4028
反应条件
sodium hydrogencarbonate; triphenylphosphine in water T=20°C; 1.5 h;
参考文献
Creencia, Evelyn Cuevas; Kosaka, Masahiro; Muramatsu, Toshikatsu; Kobayashi, Masashi; Iizuka, Tomohiro; Horaguchi, Takaaki
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 6 p. 1309 - 1317
反应条件
sulfuric acid Reflux;
参考文献
Abbasi, Muhammad Athar; Akhtar, Adnan; Aziz-Ur-Rehman; Nafeesa, Khadija; Siddiqui, Sabahat Zahra; Khan, Khalid Mohammed; Ashraf, Muhammad; Ejaz, Syeda Abida
Journal of the Chilean Chemical Society, 2013 , vol. 58, # 4 p. 2186 - 2190
参考文献
Bowman, W. Russell; Fletcher, Anthony J.; Lovell, Peter J.; Pedersen, Jan M.
Synlett, 2004 , # 11 p. 1905 - 1908
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Ni, Lijun; Li, Ziyuan; Wu, Fan; Xu, Jinyi; Wu, Xiaoming; Kong, Lingyi; Yao, Hequan
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1271 - 1274
反应条件
nitric acid T=25 - 30°C;
参考文献
Guastalla
Atti della Accademia delle Scienze di Torino, Classe di Scienze Fisiche, Matematiche e Naturali, vol. 63, p. 129
Chem. Zentralbl., 1928 , vol. 99, # II p. 984
反应条件
sulfuric acid; nitric acid in trifluoroacetic acid T=25°C; Rate constant;
参考文献
Friedlaender
Patent: ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 1, p. 125
反应条件
sulfuric acid; nitric acid in water T=25°C; nitration under var. acidic conditions discussed; Product distributionRate constant;
参考文献
Moodie, Roy B.; Schofield, Kenneth; Taylor, Peter G.; Baillie, Philip J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 842 - 847
反应条件
Rodionov reaction; 0.133333 h; Irradiation;
参考文献
Romanova; Gravis; Kudan; Bundel'
Mendeleev Communications, 2001 , vol. 11, # 1 p. 26 - 27
