1,3-二氯-2-丙醇合成路线 （共 217 条）
反应条件
MgBr2(Et2O) in diethyl ether 23 h;
参考文献
Synthesis, , # 8 p. 647 - 649
反应条件
1: With acetic acid T=110°C; 0.333333 h; 2: With hydrogenchloride 8.95 h; Product distribution / selectivity;
参考文献
WO2005/54167 A1, ;
Page/Page column 25 ;
反应条件
hydrogenchloride in toluene 14 h; Heating / reflux; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 33 ;
反应条件
hydrogenchloride T=10 - 40°C; 1 h; Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 3 p. 852 - 855
反应条件
1: With acetic acid T=110°C; 0.333333 h; 2: With hydrogenchloride 8.95 h; Product distribution / selectivity;
参考文献
WO2005/54167 A1, ;
Page/Page column 25 ;
反应条件
hydrogenchloride T=100°C; 23.75 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 33-37 ;
反应条件
boron trichloride T=-80°C; beim Behandeln des Reaktionsprodukts mit Methanol bei -80;
参考文献
Journal of the Chemical Society, , p. 348,353
反应条件
sodium hydroxide; water T=45 - 62.4°C; P=112.511 - 750.075 Torr; Product distribution / selectivity;
参考文献
WO2009/773 A1, ;
Page/Page column 19-21 ;
反应条件
ammonium fluoride; titanium tetrachloride 1) CH2Cl2, -78 deg C, 0.5h 2) ether, 78 deg C to r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 55, # 16 p. 4849 - 4852
反应条件
hydrogenchloride; sodium chloride; titanium-ruthenium oxide T=35 - 40°C; electrochemical synthesis; Product distribution;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 56, # 10 p. 2379 - 2381,2214 - 2215
