1,3,5,7-四氮杂三环[3.3.2.2(3,7)]十二烷合成路线 (共 13 条)
参考文献
Simkins; Wright
Journal of the American Chemical Society, 1955 , vol. 77, p. 3157
反应条件
in ethanol; water T=20°C; 0.25 h;
参考文献
Rivera, Augusto; Torres, Olga Lucia; Leiton, Jesus D.; Morales-Rios, Martha S.; Joseph-Nathan, Pedro
Synthetic Communications, 2002 , vol. 32, # 9 p. 1407 - 1414
反应条件
in 1,4-dioxane T=20°C;
参考文献
Rivera, Augusto; Rios-Motta, Jaime; Navarro, Miguel Angel
Heterocycles, 2006 , vol. 68, # 3 p. 531 - 537
反应条件
in water Kinetics; byproducts: 1,3,6,8-tetraazatricyclo{4.4.1.1}dodecane; Irradiation (UV/VIS); pH = 11.5, 23°C; not isolated, reaction followed by UV/VIS spectroscopy;
参考文献
Subramanian, P; Rajaram, J; Ramarkrishnan, V; Kuriacose, J C
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1991 , vol. 30, # 11 p. 913 - 919
反应条件
formic acid 10 h; Heating;
参考文献
Rivera, Augusto; Rios-Motta, Jaime
Molecules, 2007 , vol. 12, # 7 p. 1471 - 1481
反应条件
in ethanol; water T=20°C; 6 h;
参考文献
Rivera, Augusto; Torres, Olga Lucia; Leiton, Jesus D.; Morales-Rios, Martha S.; Joseph-Nathan, Pedro
Synthetic Communications, 2002 , vol. 32, # 9 p. 1407 - 1414
反应条件
in ethanol; water T=20°C; 0.25 h;
参考文献
Rivera, Augusto; Torres, Olga Lucia; Leiton, Jesus D.; Morales-Rios, Martha S.; Joseph-Nathan, Pedro
Synthetic Communications, 2002 , vol. 32, # 9 p. 1407 - 1414
反应条件
NH4F in water-d2 T=23°C; 8 h; Title compound not separated from byproducts.;
参考文献
Rivera, Augusto; Nunez, Martin E.; Avella, Eliseo; Rios-Motta, Jaime
Tetrahedron Letters, 2008 , vol. 49, # 13 p. 2154 - 2158
反应条件
acetic acid in isopropyl alcohol 1 h; Heating;
参考文献
Kuznetsov, A. I.; Vladimirova, I. A.; Basargin, E. B.; Ba, M. Kh.; Moskovkin, A. S.; Botnikov, M. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 5 p. 572 - 578
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 5 p. 675 - 680
反应条件
in ethanol; water
T=20°C; 20 h;
参考文献
Rivera, Augusto; Torres, Olga Lucia; Leiton, Jesus D.; Morales-Rios, Martha S.; Joseph-Nathan, Pedro
Synthetic Communications, 2002 , vol. 32, # 9 p. 1407 - 1414