1,1'-氧基二(环己烷)合成路线 (共 57 条)
反应条件
triethylsilane; trifluorormethanesulfonic acid in nitromethane
T=20°C; 2 h;
参考文献
Gellert, Beate A.; Kahlcke, Nils; Feurer, Markus; Roth, Stefanie
Chemistry - A European Journal, 2011 , vol. 17, # 43 p. 12203 - 12209
反应条件
trifluorormethanesulfonic acid in dichloromethane
0.3 h; Ambient temperature;
参考文献
Onaka, Makoto; Higuchi, Katsumi; Nanami, Hiroyuki; Izumi, Yusuke
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 9 p. 2638 - 2645
反应条件
palladium on activated charcoal; hydrogen
T=150°C; P=9000.9 Torr; Reagent/catalyst;
参考文献
Molinari, Valerio; Giordano, Cristina; Antonietti, Markus; Esposito, Davide
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 1758 - 1761
反应条件
triethylsilane; (+)-triethylsilyl iodide
24 h;
参考文献
Sassaman, Mark B.; Prakash, G. K. Surya; Olah, George A.
Tetrahedron, 1988 , vol. 44, # 13 p. 3771 - 3780
反应条件
1: 78 percent / I2, NO(1+)BF4(1-), O2 / CH2Cl2 / 168 h
2: 65 percent / (C4H9)3SnH / 2 h / Heating
View Scheme
参考文献
Radner, Finn
Acta Chemica Scandinavica, 1989 , vol. 43, # 9 p. 902 - 907
反应条件
hydrogen; 1 wtpercent K/1 wtpercent Pt/SiO2
T=425°C; P=5931.67 Torr;
参考文献
EXXONMOBIL CHEMICAL PATENTS INC.; XU, Teng; DAKKA, Jihad, M.; BECKER, Christopher, L.; KUECHLER, Keith, H.; BENITEZ, Francisco, M.; SMITH, Charles, M.; NAIR, Hari
Patent: WO2011/96989 A1, 2011 ;
Location in patent: Page/Page column 22-23; 25 ;
反应条件
hydrogen; 1 wtpercent K/1 wtpercent Pt/SiO2
T=425°C; P=5931.67 Torr;
参考文献
EXXONMOBIL CHEMICAL PATENTS INC.; XU, Teng; DAKKA, Jihad, M.; BECKER, Christopher, L.; KUECHLER, Keith, H.; BENITEZ, Francisco, M.; SMITH, Charles, M.; NAIR, Hari
Patent: WO2011/96989 A1, 2011 ;
Location in patent: Page/Page column 25 ;
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide
参考文献
Verzele,M. et al.
Journal of the Chemical Society, 1963 , p. 5598 - 5600
反应条件
water; MCM-22
T=119.85°C; 18 h; Product distribution; Further Variations:Catalysts;
参考文献
Nuntasri, Duangamol; Wu, Peng; Tatsumi, Takashi
Chemistry Letters, 2002 , # 2 p. 224 - 225
反应条件
palladium on activated carbon; hydrogen
T=275°C; P=75007.5 Torr; 5 h; Kinetics;
参考文献
Mortensen, Peter M.; Grunwaldt, Jan-Dierk; Jensen, Peter A.; Jensen, Anker D.
ACS Catalysis, 2013 , vol. 3, # 8 p. 1774 - 1785