2-AMINOBUTANENITRILE合成路线 （共 11 条）
参考文献
DSM N.V.
Patent: US5574181 A1, 1996 ;
参考文献
Marco, Jose L.; Ingate, Simon T.; Jaime, Carlos; Bea, Ivan
Tetrahedron, 2000 , vol. 56, # 16 p. 2523 - 2531
反应条件
ammonia 3 h; Irradiation;
参考文献
Guillemin, Jean-Claude; Breneman, Curt M.; Joseph, Jeffrey C.; Ferris, James P.
Chemistry - A European Journal, 1998 , vol. 4, # 6 p. 1074 - 1082
反应条件
ammonium chloride in diethyl ether
参考文献
Jenni,J. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 1163 - 1171
参考文献
Strack; Fanselow
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1929 , vol. 180, p. 158
反应条件
ammonium chloride 1.) water, 0 deg C, 5 min 2.) water, 20 min, RT; Yield given. Multistep reaction;
参考文献
Guillemin, Jean-Claude; Denis, Jean-Marc
Tetrahedron, 1988 , vol. 44, # 14 p. 4431 - 4446
参考文献
Kurtz,P.; Disselnkoetter,H.
Justus Liebigs Annalen der Chemie, 1972 , vol. 764, p. 69 - 93
反应条件
Achromobacter obae α-amino-ε-caprolactam racemase; Brevundimonas diminuta TPU 5720 L-amino acid amidase; Rhodococcus opacus 71D nitrile hydralase; pyridoxal 5'-phosphate in potassium phosphate buffer T=30°C; pH=7; 3 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Yasukawa, Kazuyuki; Hasemi, Ryuji; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 13 p. 2328 - 2332
反应条件
potassium hydroxide
P=0.004 Torr; 1.) 2 h, 300 deg C 2.) 2 h, 50 deg C; Yield given;
参考文献
Guillemin, Jean-Claude; Denis, Jean-Marc
Tetrahedron, 1988 , vol. 44, # 14 p. 4431 - 4446
参考文献
Strack; Fanselow
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1929 , vol. 180, p. 158
