1: With dimethylsulfide borane complex in diethyl ether; pentane T=0°C; 0.75 h; 2: With hydrogenchloride in diethyl ether; water; pentane T=20°C; 1.5 h;
参考文献
THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY, DEPARTMENT OF HEALTH AND HUMAN SERVICES
Patent: WO2009/29844 A1, 2009 ;
Location in patent: Page/Page column 38-39 ;