1-(4-吗啉)-2-苯基乙烷硫酮合成路线 （共 33 条）
反应条件
sodium hydroxide 0.0166667 h; microwave irradiation;
参考文献
Matloubi Moghaddam; Ghaffarzadeh
Synthetic Communications, 2001 , vol. 31, # 2 p. 317 - 321
反应条件
hydrogenchloride 1.) ether, room temp., 4h; Yield given. Multistep reaction;
参考文献
Tominaga, Yoshinori; Kohra, Shinya; Hosomi, Akira
Tetrahedron Letters, 1987 , vol. 28, # 14 p. 1529 - 1532
参考文献
Baddiley
Journal of the Chemical Society, 1950 , p. 3693
反应条件
beim anschliessenden Erwaermen des Reaktionsprodukts mit wss. NaOH;
参考文献
Hager; Kramer
Journal of the American Pharmaceutical Association (1912-1977), 1955 , vol. 44, p. 649,652
反应条件
MCM-41 mesoporous silica in ethanol; water
T=80 - 90°C; 7 h; Green chemistry;
参考文献
Ray, Suman; Bhaumik, Asim; Dutta, Arghya; Butcher, Ray J.; Mukhopadhyay, Chhanda
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2164 - 2170
反应条件
silica gel-supported tetrafluoroboric acid; sulfur
T=80°C; Willgerodt-Kindler reaction; 0.75 h; Neat (no solvent);
参考文献
Salim, Suresh D.; Pathare, Sagar P.; Akamanchi, Krishnacharya G.
Catalysis Communications, 2011 , vol. 13, # 1 p. 78 - 81
反应条件
Na2S*9H2O in N,N-dimethyl-formamide
T=80°C; 8 h; Sealed tube;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Li, Jianxiao
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 4 p. 700 - 707
参考文献
The Goodyear Tire and Rubber Company
Patent: US5019611 A1, 1991 ;
反应条件
sulfur
T=120°C; 40 h; Inert atmosphere; chemoselective reaction;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 16 p. 4274 - 4277
反应条件
sulfur
Willgerodt-Kindler reaction; 0.0666667 h; microwave irradiation;
参考文献
Darabi, Hossein Reza; Aghapoor, Kioumars; Tabar-Heydar, Kourosh; Nooshabadi, Masoud
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1189 - 1192
