1,1,1,2-四氟乙烷合成路线 （共 120 条）
反应条件
fluorinated gallium(III) oxide Ambient temperaturefurther reagent: fluorinated indium(III) oxide; Product distribution;
参考文献
Journal of the Chemical Society - Faraday Transactions, , vol. 94, # 13 p. 1881 - 1885
参考文献
Trans.electroch.Soc.Chem.Abstr., vol. 95, p. 60
Trans.electroch.Soc.Chem.Abstr., , p. 2876
反应条件
in diethyl ether; hexane T=-78 - 20°C; Addition; Title compound not separated from byproducts;
参考文献
Burdon; Coe; Haslock; Powell
Journal of Fluorine Chemistry, 1999 , vol. 99, # 2 p. 127 - 131
反应条件
T=1006.9°C; gas-phase reaction, thermal and thermooxidative stability, various degree of adiabatic compression or various maximum temperature in adiabatic compression pulse, oxygen presence or absence; Product distributionMechanismKinetics;
参考文献
Buravtsev, N. N.; Grigor'ev, A. S.; Kolbanovskii, Yu. A.; Ovsyannikov, A. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1880 - 1890
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1794 - 1801
反应条件
n-butyllithium; iodine in diethyl ether; hexane 1.) -78 deg C;
参考文献
Burdon, James; Coe, Paul L.; Haslock, Iain B.; Powell, Richard L.
Chemical Communications, 1996 , # 1 p. 49 - 50
反应条件
in diethyl ether T=-78 - 20°C; Addition; Title compound not separated from byproducts;
参考文献
Burdon; Coe; Haslock; Powell
Journal of Fluorine Chemistry, 1999 , vol. 99, # 2 p. 127 - 131
反应条件
n-butyllithium in diethyl ether; hexane 1.) -78 deg C;
参考文献
Burdon, James; Coe, Paul L.; Haslock, Iain B.; Powell, Richard L.
Chemical Communications, 1996 , # 1 p. 49 - 50
反应条件
1: 1,1,1-trifluoro-2-fluoroethane With zinc(II) chloride; lithium diisopropyl amide in tetrahydrofuran T=15 - 20°C; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=65°C; 3 h;
参考文献
Raghavanpillai, Anilkumar; Burton, Donald J.
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7083 - 7091
反应条件
n-butyllithium in diethyl ether; hexane 1.) -78 deg C;
参考文献
Burdon, James; Coe, Paul L.; Haslock, Iain B.; Powell, Richard L.
Chemical Communications, 1996 , # 1 p. 49 - 50
反应条件
fluorine T=-20°C; Fluorination; 0.4 h; Title compound not separated from byproducts;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
