2-苯基-2,4,6-三羟基苯乙酮合成路线 （共 16 条）
反应条件
1: With hydrogenchloride; zinc(II) chloride in diethyl ether T=0 - 20°C; 2: With water in methanol 5 h; Reflux;
参考文献
Ng, Lean-Teik; Ko, Horng-Huey; Lu, Tzy-Ming
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 13 p. 4360 - 4366
反应条件
hydrogenchloride; carbon disulfide; aluminium trichloride in water; nitrobenzene
反应条件
aluminium trichloride in nitrobenzene T=20 - 60°C; 2 h;
参考文献
Lin, Chun-Mao; Huang, Sheng-Tung; Lee, Fu-Wei; Kuo, Hsien-Saw; Lin, Mei-Hsiang
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 13 p. 4402 - 4409
反应条件
aluminium trichloride in anhydrous dichloroethane
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Bulletin de la Societe Chimique de France, , p. 2309 - 2322
反应条件
zinc(II) chloride; trichlorophosphate 24 h; Ambient temperature;
参考文献
Devi, Nirada; Jain, Niveta; Krishnamurty, H. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 8 p. 874 - 875
反应条件
potassium carbonate; acetone Behandeln des Reaktionsprodukts mit wss. Natronlauge;
参考文献
Gilbert et al.
Journal of the Chemical Society, 1957 , p. 3740,3745
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Kariyone; Inagaki
Yakugaku Zasshi, 1949 , vol. 69, p. 431
Chem.Abstr., 1950 , p. 3457
反应条件
boron trifluoride diethyl etherate in DMF (N,N-dimethyl-formamide) T=50 - 95°C; 1 h;
参考文献
CHIESI FARMACEUTICI S.p.A.
Patent: EP1229036 A1, 2002 ;
Location in patent: Page 9 ;
反应条件
1: With boron trifluoride diethyl etherate; methanesulfonyl chloride T=100°C; 2: With water
参考文献
Mrug; Bondarenko; Khilya; Frasinyuk
Chemistry of Natural Compounds, 2013 , vol. 49, # 2 p. 235 - 241
Khim. Prir. Soedin., 2013 , # 2 p. 203 - 208,6
