5-硝基苯并呋喃-2-羧酸乙酯合成路线 （共 19 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=85 - 90°C; 15 h; Inert atmosphere;
参考文献
WO2013/153492 A2, ;
Page/Page column 23 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=130°C; 6 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 14 p. 4939 - 4946
反应条件
potassium hydroxide in 1,4-dioxane 1 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 10 p. 2821 - 2825
参考文献
Journal of the Chemical Society, , vol. 123, p. 3381
参考文献
Journal of the Chemical Society, , vol. 123, p. 3381
反应条件
sulfuric acid; nitric acid; acetic anhydride
参考文献
Nippon Kagaku Zasshi, , vol. 73, p. 282,285
Chem.Abstr., , p. 9957
反应条件
potassium carbonate; butanone
参考文献
Nippon Kagaku Zasshi, , vol. 73, p. 282,285
Chem.Abstr., , p. 9957
Gazzetta Chimica Italiana, , vol. 86, p. 1257,1267
反应条件
1: ethanolic KOH-solution 2: copper; quinoline 3: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Tanaka
Nippon Kagaku Zasshi, 1952 , vol. 73, p. 282,285
Chem.Abstr., 1953 , p. 9957
反应条件
lithium borohydride in methanol T=20°C; 4 h;
参考文献
RIGEL PHARMACEUTICALS, INC.
Patent: WO2007/30680 A2, 2007 ;
Location in patent: Page/Page column 167-168 ;
WO 2007/030680 A2
参考文献
Tanaka
Nippon Kagaku Zasshi, 1952 , vol. 73, p. 282,285
Chem.Abstr., 1953 , p. 9957
Full Text Show Details
Andrisano et al.
Gazzetta Chimica Italiana, 1956 , vol. 86, p. 1257,1267
