3,3-二甲基-1-苯基-2-丁酮合成路线 (共 50 条)
反应条件
gold(III) chloride; silver hexafluoroantimonate in 1,4-dioxane
T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Gudla, Vanajakshi; Balamurugan, Rengarajan
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5243 - 5247
反应条件
tri-n-butyltin methoxide; bis (triortho-tolylphosphine)palladium(II) chloride in toluene
T=100°C; 5 h;
参考文献
Kosugi, Masanori; Hagiwara, Isao; Sumiya, Takashi; Migita, Toshihiko
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 344 - 345
反应条件
carbon monoxide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in tetrahydrofuran
T=120°C; 24 h;
参考文献
Nishiyama, Yutaka; Inoue, Jun; Teranishi, Kazuyo; Moriwaki, Masami; Hamanaka, Sawako
Tetrahedron Letters, 1992 , vol. 33, # 42 p. 6347 - 6350
反应条件
sodium ethanolate in ethanol
T=50°C; Substitution; 72 h;
参考文献
Angle, Steven R.; Neitzel, Martin L.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6458 - 6461
反应条件
copper(I) bromide in tetrahydrofuran
T=20°C; 1 h;
参考文献
Piazza, Claudia; Millot, Nicolas; Knochel, Paul
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 88 - 95
反应条件
cerium(III) chloride in tetrahydrofuran
T=-78°C; 16 h;
参考文献
Ahn, Yoonmo; Cohen, Theodore
Tetrahedron Letters, 1994 , vol. 35, # 2 p. 203 - 206
反应条件
magnesium in (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
Bayer Aktiengesellschaft
Patent: US4048318 A1, 1977 ;
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
0.75 h; Heating;
参考文献
Hamann, Blake C.; Hartwjg, John F.
Journal of the American Chemical Society, 1997 , vol. 119, # 50 p. 12382 - 12383
反应条件
potassium tert-butylate; ammonia; iron(II) sulfate
other ketone enolate ions, diethyl phosphite ion;
参考文献
Galli, Carlo; Bunnett, J. F.
Journal of Organic Chemistry, 1984 , vol. 49, # 16 p. 3041 - 3042
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; tri-n-butyltin fluoride in benzene
24 h; Heating;
参考文献
Kuwajima, Isao; Urabe, Hirokazu
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6831 - 6833