乙基三甲基硅基缩三甲基硅基乙烯酮合成路线 （共 14 条）
反应条件
tetra-n-butylammonium acetate in dichloromethane T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
tetra-n-butylammonium acetate in dichloromethane T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
tetra-n-butylammonium acetate in dichloromethane T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
anhydrous lithium acetate in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
anhydrous lithium acetate in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
tetra-n-butylammonium acetate in dichloromethane T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
tetra-n-butylammonium acetate in dichloromethane T=0°C; 1 h;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
lithium diisopropyl amide
1.) -78 deg C, 3 h; 2.) RT, 1.5 h;
参考文献
Matsuda, Isamu
Journal of Organometallic Chemistry, 1987 , vol. 321, p. 307 - 316
反应条件
1: trimethylsilyl acetic acid ethyl ester With lithium diisopropyl amide in tetrahydrofuran
T=-78°C;
2: tert-butyldimethylsilyl chloride in tetrahydrofuran
T=-78°C; Further stages.;
参考文献
Michida, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 2008 , vol. 37, # 7 p. 704 - 705
反应条件
triethylamine in diethyl ether
2 h; Ambient temperature; Yields of byproduct given;
参考文献
Emde, Herbert; Simchen, Gerhard
Liebigs Annalen der Chemie, 1983 , # 5 p. 816 - 834
