反应条件
1: [RuIII(2,4-pentanedionato)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane; methanesulfonic acid; hydrogen / tetrahydrofuran / 16 h / 220 °C / 30003 Torr / |Autoclave; |Inert atmosphere 2: triethylamine / dichloromethane / 0 - 20 °C 3: [RuIII(2,4-pentanedionato)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane; methanesulfonic acid; hydrogen / tetrahydrofuran / 16 h / 220 °C / 7500.75 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 33 p. 11039 - 11050