1,3-二(二甲氨基)-2-丙醇合成路线 (共 10 条)
反应条件
ethanol T=115 - 120°C;
参考文献
Journal of the Chemical Society, , p. 172
参考文献
Journal of Organic Chemistry, , vol. 14, p. 346,349
反应条件
T=60°C; im geschlossenen Rohr;
参考文献
Chemische Berichte, , vol. 17, p. 511
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 239, p. 284
参考文献
Gazzetta Chimica Italiana, , vol. 63, p. 753
参考文献
Gazzetta Chimica Italiana, , vol. 63, p. 753
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 239, p. 284
反应条件
1: methacrylic acid methyl ester With (10H)-phenothiazine; tris(nonylphenyl)phosphite; 1,4-dimethoxy benzene T=96°C; P=760.051 Torr; Heating / reflux; 2: With oxygen; lithium oxide T=121°C; 1.66667 h; 3: N,N,N',N'-tetramethyl-2-hydroxy-1,3-propanediamine T=107 - 112°C; 5 - 6 h; Product distribution / selectivity;
参考文献
Taminco N.V.
Patent: EP1512676 A1, 2005 ;
Location in patent: Page/Page column 7-8 ;
反应条件
(10H)-phenothiazine; sodium methylate in methanol
参考文献
Korshunov,M.A. et al.
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, # 11 p. 1947 - 1952,1893 - 1898
参考文献
Milton, John; Vicker, Nigel; Folkes, Adrian; Wang, Shouming; Denny, William Alexander
Patent: US2003/139409 A1, 2003 ;