1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=25°C; 1.5 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 29 p. 12281 - 12288
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=25°C; 1.5 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 29 p. 12281 - 12288
chloro-trimethyl-silane; zinc in dichloromethane 0.0833333 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
Titanium substituted ZSM-5; dihydrogen peroxide in butanone T=80°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Catalysis, , vol. 149, # 1 p. 195 - 205
