苯甲醛乙烷-1,2-二基二硫代缩醛合成路线 (共 29 条)
反应条件
2,2'-azo-bisisobutyronitrile in neat (no solvent) T=80°C; 1.5 h; Product distribution;
参考文献
Gutierrez, Carlos G.; Stringham, Rex A.; Nitasaka, Tadashi; Glasscock, Karl G.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3393 - 3395
反应条件
1: CH2Cl2 / Ambient temperature 2: CsF / CH2Cl2 / 26 h / Heating View Scheme
参考文献
Ichikawa, Junji; Sugimoto, Ken-ichi; Sonoda, Takaaki; Kobayashi, Hiroshi
Chemistry Letters, 1987 , p. 1985 - 1988
反应条件
T=769.9°C; Curie-point pyrolysis; Product distribution;
参考文献
Hoffmann, Reinhard W.; Barth, Wolfgang; Carlsen, Lars; Egsgaard, Helge
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1687 - 1692
反应条件
methyloxirane in 1,2-dichloro-ethane 1 h; Heatingother 2-mono- and 2,2-disubstituted 1,3-dithiolanes; Product distribution;
参考文献
Heterocycles, , vol. 22, # 5 p. 1053 - 1056
反应条件
methyloxirane in 1,2-dichloro-ethane 1 h; Heatingother 2-mono- and 2,2-disubstituted 1,3-dithiolanes; Product distribution;
参考文献
Heterocycles, , vol. 22, # 5 p. 1053 - 1056
反应条件
N-bromosuccinmide T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
N-bromosuccinmide T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
T=769.9°C; Curie-point pyrolysis; Product distribution;
参考文献
Hoffmann, Reinhard W.; Barth, Wolfgang; Carlsen, Lars; Egsgaard, Helge
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1687 - 1692
反应条件
thionyl chloride; silica gel in benzene
T=20°C; 5 h;
参考文献
Pandey, Lokesh Kumar; Pathak, Uma; Tank, Rekha; Mazumder, Avik
Heterocyclic Communications, 2009 , vol. 15, # 3 p. 167 - 171
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677