反应条件
in tetrachloromethane under N2; mixt. of WCl6 (3.26 mmol), CCl4 (1.63 mmol) and Bi (4.35 mmol)heated in evacuated and sealed Pyrex ampule in tube furnace at 400.degr ee.C for 3 days; sublimation of BiCl3 at 360°C;
参考文献
Welch, Eric J.; Crawford, Nathan R. M.; Bergman, Robert G.; Long, Jeffrey R.
Journal of the American Chemical Society, 2003 , vol. 125, # 38 p. 11464 - 11465
