8-甲基-1,2,3,4-四氢喹啉合成路线 (共 15 条)
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol T=40°C; P=760.051 Torr; 3 h;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr; 12 h; Ambient temperature;
参考文献
Meyers, A. I.; Himmelsbach, Richard J.; Reuman, Michael
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4053 - 4058
反应条件
1: 92 percent / DIBAL / toluene / 12 h / Ambient temperature 2: 78 percent / H2 / Pd/C / ethanol / 12 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Meyers, A. I.; Himmelsbach, Richard J.; Reuman, Michael
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4053 - 4058
反应条件
hydrogen; platinum(IV) oxide in trifluoroacetic acid
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
palladium 10 on activated carbon; zinc T=150°C; 40 h; Autoclave;
参考文献
Abarca, Belen; Adam, Rosa; Ballesteros, Rafael
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 9 p. 1826 - 1833
反应条件
hydrogen; nickel T=200°C; P=7600 Torr; or Ru/C, 100 atm, 150 deg C; Equilibrium constant;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174
反应条件
hydrogen; nickel T=200°C; P=7600 Torr; or Ru/C, 100 atm, 150 deg C; Rate constant;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174
参考文献
Pinkus
Chemische Berichte, 1892 , vol. 25, p. 2802
参考文献
Avramoff; Sprinzak
Journal of Organic Chemistry, 1957 , vol. 22, p. 571,573
参考文献
Bamberger; Wulz
Chemische Berichte, 1891 , vol. 24, p. 2051
Full Text Show Details
Ziegler
Chemische Berichte, 1888 , vol. 21, p. 866