2-(甲基苯基)氨基甲酸乙酯合成路线 （共 17 条）
反应条件
phosphorus pentoxide
参考文献
Nevile; Winther
Chemische Berichte, 1879 , vol. 12, p. 2325
反应条件
hydrazine T=120°C; 16 h; Neat (no solvent);
参考文献
BAYER CROPSCIENCE AKTIENGESELLSCHAFT
Patent: WO2005/58838 A1, 2005 ;
Location in patent: Page/Page column 67 ;
反应条件
T=230 - 240°C; 0.5 h;
参考文献
Hassan, Alaa A; Mourad, Aboul-fetouh E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 277 - 279
Title/Abstract Full Text Show Details
Hassan, Alaa A.; Mourad, Aboul-Fetouh E.
Revue Roumaine de Chimie, 1994 , vol. 39, # 4 p. 397 - 404
反应条件
tin; ammonium chloride in methanol
T=25°C; 2 h; Sonication;
参考文献
Chandrasekhar; Narsihmulu; Jagadeshwar
Synlett, 2002 , # 5 p. 771 - 772
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
T=0 - 20°C; 3 h;
参考文献
BAYER CROPSCIENCE AKTIENGESELLSCHAFT
Patent: WO2005/58838 A1, 2005 ;
Location in patent: Page/Page column 67 ;
反应条件
[Pt(triphenylphosphine)2Cl2]; tin(IV) chloride; triethylamine
T=180°C; P=45600 Torr; 4 h;
参考文献
Watanabe; Tsuji; Takeuchi; Suzuki
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 11 p. 3343 - 3348
参考文献
Nevile; Winther
Chemische Berichte, 1879 , vol. 12, p. 2325
Full Text Show Details
Cosack
Chemische Berichte, 1879 , vol. 12, p. 1450
Chemische Berichte, 1880 , vol. 13, p. 1090
Full Text Show Details
Lachmann
Chemische Berichte, 1879 , vol. 12, p. 1350
反应条件
1: 1-tert-butyl-1-isopropyl-3-phenylurea With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane
T=0°C; 3 h; Inert atmosphere;
2: ethanol; methyl iodide in diethyl ether; hexane
T=0°C; Inert atmosphere;
参考文献
Houlden, Chris E.; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2010 , vol. 12, # 13 p. 3090 - 3092
反应条件
trifluoroacetic acid
T=109°C; 2 h;
参考文献
Takeuchi, Hiroshi; Mastubara, Eiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 5 p. 981 - 985
反应条件
1: chloroform; chlorine
2: potash
View Scheme
参考文献
Lachmann
Chemische Berichte, 1879 , vol. 12, p. 1349
