反应条件
1.1: hydroxylamine hydrochloride; triethylamine / dichloromethane / 2 h / 0 - 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
3.1: tetrabutyl ammonium fluoride / acetonitrile / 0.1 h / 80 °C
3.2: 0.08 h / 80 °C
View Scheme
参考文献
Lee, Jin Young; Lee, Yong Han; Byun, Yong Gwan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 641 - 649