(三甲基硅基)乙酸乙酯合成路线 (共 118 条)
反应条件
zinc in diethyl ether
参考文献
Albaugh-Robertson, Pamela; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5288 - 5302
参考文献
Gold; Sommer; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2874
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Gmelin Handbook: Si: MVol.C, 4, page 14 - 18
反应条件
in diethyl ether dropwise addn. of (CH3)3SiCl to a (C6H5)3CNa-CH3COOC2H5-mixt. in ether;;
参考文献
Hance; Hauser
Journal of the American Chemical Society, 1953 , vol. 75, p. 994
反应条件
1: ethyl acetate With lithium diisopropyl amide 2: chloro-trimethyl-silane in tetrahydrofuran T=-78 - -40°C; Further stages. Title compound not separated from byproducts.;
参考文献
Harada, Toshiro; Egusa, Takayuki; Igarashi, Yasuto; Kinugasa, Motoharu; Oku, Akira
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7080 - 7090
反应条件
carboxylic acid in dichloromethane further solvent: (CH2)2Cl2;
参考文献
Shchukovskaya,L.L. et al.
Doklady Chemistry, 1965 , vol. 164, p. 887 - 890
Doklady Akademii Nauk SSSR, 1965 , vol. 164, # 2 p. 357 - 360
反应条件
triethylamine in diethyl ether 2 h; Ambient temperature; Yields of byproduct given;
参考文献
Emde, Herbert; Simchen, Gerhard
Liebigs Annalen der Chemie, 1983 , # 5 p. 816 - 834
反应条件
ytterbium(III) triflate in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Makioka, Yoshikazu; Taniguchi, Yuki; Takaki, Ken; Fujiwara, Yuzo
Chemistry Letters, 1994 , # 3 p. 645 - 648
参考文献
Semenova,N.V.; Komarov,N.V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1972 , vol. 21, p. 177 - 179
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1972 , vol. 21, p. 185 - 187
反应条件
1: Hg(OAc)2, H2SO4 2: H2 / Raney-Ni View Scheme
参考文献
Semenova,N.V.; Komarov,N.V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1972 , vol. 21, p. 177 - 179
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1972 , vol. 21, p. 185 - 187
参考文献
Schmidt,U.; Schwochau,M.
Tetrahedron Letters, 1967 , p. 875 - 879