反应条件
tetraehtylammonium perchlorate in acetonitrile
Electrochem. Process; electrochemical process with Pb anode suspended into soln. of thiol, -10°C for 5 h, N2 atm.; washing a ppt. with petroleum ether, drying; elem. anal.;
参考文献
Hencher, J. Lawrence; Khan, Masood; Said, Farouq F.; Sieler, Robert; Tuck, Dennis G.
Inorganic Chemistry, 1982 , vol. 21, p. 2787 - 2791