4-乙酰氧基-2-氮杂环丁酮合成路线 （共 46 条）
反应条件
sodium hydroxide in water
参考文献
Prasad, Kapa; Schulz, Gerhard; Hamberger, Helmut; Stuetz, Peter
Heterocycles, 1982 , vol. 19, # 2 p. 291 - 295
反应条件
sodium hydroxide in 1,4-dioxane; water
参考文献
Prasad, Kapa; Schulz, Gerhard; Hamberger, Helmut; Stuetz, Peter
Heterocycles, 1982 , vol. 19, # 2 p. 291 - 295
反应条件
potassium hydroxide T=25°C; MechanismRate constant;
参考文献
Fedor, Leo R.
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5094 - 5097
反应条件
zinc diacetate in benzene
20 h; Heating;
参考文献
Basak; Khamrai
Synthetic Communications, 1994 , vol. 24, # 2 p. 131 - 135
反应条件
sodium hydroxide in ethanol
1) -10 deg C, 30 min; 2) 0 deg C, 1 h;
参考文献
Pfaendler, H. R.; Gosteli, J.; Woodward R. B.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2039 - 2043
反应条件
sodium hydroxide; trifluoroacetic acid in ethanol; dichloromethane; chloroform
参考文献
Ciba-Geigy Corporation
Patent: US4436661 A1, 1984 ;
反应条件
Cu(I)Br*SMe2
1.) ether, -20 degC, 15 min; 2.) -50 degC, 30 min; Yield given. Multistep reaction;
参考文献
Hua, Duy H.; Verma, Akhilkumar
Tetrahedron Letters, 1985 , vol. 26, # 5 p. 547 - 550
参考文献
Kobayashi, Takeo; Ishida, Nobory; Hiraoka, Tetsuo
Journal of the Chemical Society, Chemical Communications, 1980 , # 15 p. 736 - 737
反应条件
zinc(II) iodide in dichloromethane
2 h; Ambient temperature;
参考文献
Reider; Rayford; Grabowski
Tetrahedron Letters, 1982 , vol. 23, # 4 p. 379 - 382
反应条件
diethylaluminium chloride; zinc in tetrahydrofuran
T=-10 - -5°C; 1 h;
参考文献
Oida; Yoshida; Ohki
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3494 - 3500
