1,1,2-三甲氧基乙烷合成路线 （共 14 条）
反应条件
methanol; cobalt catalyst; hydrogen T=160 - 170°C; P=441305 Torr;
反应条件
tris (2,4-dibromophenyl)amine; sodium methylate; lithium perchlorate T=40°C; electrochem. oxidation;
参考文献
Ginzel, Klaus-Dieter; Steckhan, Eberhard; Degner, Dieter
Tetrahedron, 1987 , vol. 43, # 24 p. 5797 - 5806
参考文献
Chemische Berichte, , vol. 63, p. 422 Anm.14
反应条件
SnCl2·2H2O in methanol Large scale; Reagent/catalystTemperatureTime;
参考文献
Catalysis Communications, , vol. 49, p. 78 - 81
反应条件
potassium hydroxide (electrolysis);
参考文献
Canadian Journal of Chemistry, , vol. 47, p. 2117 - 2118
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1570 - 1572
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1685 - 1688
反应条件
toluene-4-sulfonic acid Substitution; Heating;
参考文献
Taskinen, Esko
Magnetic Resonance in Chemistry, 1998 , vol. 36, # 8 p. 573 - 578
反应条件
ozone in ethyl acetate T=-78°C; Rate constant;
参考文献
Taillefer, Roland J.; Thomas, Shirley E.; Nadeau, Yves; Fliszar, S.; Henry, Herve
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1138 - 1143
反应条件
(i) COCl2, (ii) aq. K2CO3; Multistep reaction;
参考文献
Pluempe,H.; Schegk,E.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1967 , vol. 300, p. 704 - 708
反应条件
1: 2-methoxyacetaldehyde dimethyl acetal With phosphorus pentachloride T=20 - 60°C; 1.25 h; 2: N,N-dimethyl-formamide T=70°C; 0.75 h; 3: GNO3 With sodium hydroxide in methanol T=0 - 100°C; 1.75 h;
参考文献
VIVALIS; GUEDAT, Philippe; BERECIBAR, Amaya; CIAPETTI, Paola; VENKATA PITHANI, Subhash; TROUCHE, Nathalie
Patent: WO2013/171281 A1, 2013 ;
Location in patent: Page/Page column 109-110 ;
