(1S,2r)-2-溴环己醇合成路线 （共 20 条）
反应条件
1: glacial acetic acid; water / 100 - 110 °C 2: aq.-ethanolic NaOH View Scheme
参考文献
Winstein; Buckles
Journal of the American Chemical Society, 1942 , vol. 64, p. 2780,2784
反应条件
1: 66.6 percent / diethylaminosulfur trifluoride / CH2Cl2 / 1.5 h / -78 °C 2: 47 percent / sodamide / 2-methyl-propan-2-ol; tetrahydrofuran View Scheme
参考文献
Hudlicky,H.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 441
反应条件
1: 95 percent / pyridine / 24 h / Ambient temperature 2: 84 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 3 h / 120 °C View Scheme
参考文献
Gupta, Ajay K.; Kazlauskas, Romas J.
Tetrahedron: Asymmetry, 1993 , vol. 4, # 5 p. 879 - 888
参考文献
Cristol et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 598,599
反应条件
water; acetic acid T=100 - 110°C;
参考文献
Winstein; Buckles
Journal of the American Chemical Society, 1942 , vol. 64, p. 2780,2784
反应条件
1: H2SO4 2: acetic acid anhydride; glacial acetic acid / 100 - 110 °C View Scheme
参考文献
Winstein; Buckles
Journal of the American Chemical Society, 1942 , vol. 64, p. 2780,2784
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1600
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1600
参考文献
Brown; Gedye; Slebocka-Tilk; Buschek; Kopecky
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4515 - 4521
反应条件
1: 66.6 percent / diethylaminosulfur trifluoride / CH2Cl2 / 1.5 h / -78 °C
2: 62.5 percent / methanol / Heating
View Scheme
参考文献
Hudlicky,H.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 441
