2,4,6-三乙基-1,3,5-三氧杂环己烷合成路线 （共 9 条）
反应条件
[P(2-pyridyl)3W(CO)(NO)2](2+)(BF4(1-))2 T=20°C; 24 h;
参考文献
Wang, Hsing-Shiun; Yu, Shuchun Joyce
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 1051 - 1055
反应条件
boron trifluoride diethyl etherate in dichloromethane Title compound not separated from byproducts.;
参考文献
Griesbeck, Axel G.; El-Idreesy, Tamer T.; Fiege, Maren; Brun, Reto
Organic Letters, 2002 , vol. 4, # 24 p. 4193 - 4195
参考文献
Chemische Werke Huels, A.G.
Patent: US4330474 A1, 1982 ;
反应条件
boron trifluoride diethyl etherate; ammonium chloride in dichloromethane Ar; -78°C; slow addn. of BF3*Et2O; after 1 h hydrolysed with NH4Cl/H2O at room temp.;; work up at -30°C; aq. layer extd. with Et2O; combined organic layers dried over Na2SO4; evapd.;;
参考文献
Mitchell, Terence N.; Schneider, Ulrich; Heesche-Wagner, Kerstin
Journal of Organometallic Chemistry, 1991 , vol. 411, # 1-2 p. 107 - 120
反应条件
sulfided Ni-Mo; hydrogen T=180°C; P=51714.8 Torr; Product distribution; Further Variations:TemperaturesReagentsspace velocity;
参考文献
Wang, Xueqin; Saleh, Ramzi Y.; Ozkan, Umit S.
Journal of Catalysis, 2005 , vol. 231, # 1 p. 20 - 32
反应条件
n-butyl(crotyl)tin dichloride Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Gambaro, Alessandro; Boaretto, Andrea; Marton, Daniele; Tagliavini, Giuseppe
Journal of Organometallic Chemistry, 1983 , vol. 254, # 3 p. 293 - 304
反应条件
in water-d2 T=25°C; Equilibrium constantMechanismKinetics; Temperature;
参考文献
Corrochano, Pablo; Garcia-Rio, Luis; Poblete, Francisco Javier; Rodriguez-Dafonte, Pedro
Tetrahedron Letters, 2010 , vol. 51, # 13 p. 1761 - 1765
反应条件
in water T=110°C; 3 h; addition of triglyceride, variation of solvent conditions; Product distribution;
参考文献
Okumura, Joji
Agricultural and Biological Chemistry, 1991 , vol. 55, # 6 p. 1537 - 1545
反应条件
T=-5°C; Versetzen des Reaktionsgemisches mit absol. Alkohol;
参考文献
Monatshefte fuer Chemie, , vol. 48, p. 252
