2-[(二甲基氨基)甲基]-6-甲基苯酚合成路线 (共 7 条)
反应条件
potassium carbonate in toluene 5 h; Ambient temperature;
参考文献
Pochini, Andrea; Puglia, Giuseppe; Ungaro, Rocco
Synthesis, 1983 , # 11 p. 906 - 907
参考文献
Epstein,J. et al.
Journal of the American Chemical Society, 1964 , vol. 86, p. 4959 - 4963
反应条件
in acetonitrile T=80°C;
参考文献
Baires, S. V.; Ivanov, V. B.; Ivanov, B. E.; Zyablikova, T. A.; Efrimov, Yu. Ya.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 9 p. 1881 - 1884
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 9 p. 2030 - 2033
反应条件
hydrogen tetrachloroaurate(III) trihydrate; trichloromonobromomethane in dichloromethane T=20°C; Inert atmosphere; Overall yield = 62 percent;
参考文献
Sun, Wenbo; Lin, Huacan; Zhou, Wenyu; Li, Zigang
RSC Advances, 2014 , vol. 4, # 15 p. 7491 - 7494
参考文献
Decombe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1933 , vol. 196, p. 866
参考文献
Carlin; Landerl
Journal of the American Chemical Society, 1950 , vol. 72, p. 2762
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Azuma et al.
Kogyo Kagaku Zasshi, 1958 , vol. 61, p. 1035,1036
Chem.Abstr., 1961 , p. 27187
反应条件
in N,N-dimethyl-formamide 24 h; Heating;
参考文献
Balasubramanian,K.K.; Selvaraj,S.
Synthesis, 1977 , p. 767