4-硝基苯基-1,3-恶噻戊环合成路线 (共 10 条)
反应条件
iodine in water T=20°C; 0.416667 h;
参考文献
Bandgar; Bettigeri, Sampada V.
Journal of Chemical Research, 2004 , # 6 p. 389 - 391
反应条件
methyltrichloromonosilane T=20°C; 0.5 h; Neat (no solvent);
参考文献
Laskar, Rajibul A.; Begum, Naznin A.; Mir, Mohammad Hedayetullah; Rohman, Md. Rumum; Khan, Abu T.
Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5839 - 5844
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one in chloroform 0.583333 h; Heating;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza; Zolfigol
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1047 - 1071
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane 0.0833333 h; Ambient temperaturedeprotection of carbonyl compounds by -SCH2CH2O- uptake; Product distribution;
参考文献
Ravindranathan, T.; Chavan, Subhash P.; Varghese, Jos P.; Dantale, Shubhada W.; Tejwani, Rajkumar B.
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1937 - 1938
反应条件
bromine; dimethyl sulfoxide in chloroform T=20°C; 0.0666667 h;
参考文献
Rohman, Md. Rumum; Rajbangshi, Mantu; Laloo, Badaker M.; Sahu, Priti R.; Myrboh, Bekington
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2862 - 2864
反应条件
potassium superoxide; tetraethylammonium bromide in N,N-dimethyl-formamide T=20°C; 2.5 h;
参考文献
Singh, Satish Kumar; Singh, Krishna Nand
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 9 p. 2339 - 2343
反应条件
N-bromosuccinmide in dichloromethane T=20°C; 0.166667 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
potassium superoxide; tetraethylammonium bromide in N,N-dimethyl-formamide T=20°C; 2.5 h;
参考文献
Singh, Satish Kumar; Singh, Krishna Nand
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 9 p. 2339 - 2343
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.166667 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
2,4,6-trichloro-1,3,5-triazine; C6H5C(CH3)O(CH2)2S in N,N-dimethyl-formamide
T=20°C; 0.5 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71