1,2,2,2-四氟乙基磺酰氯合成路线 (共 16 条)
参考文献
Asahi Glass Company, Limited
Patent: US2012/165571 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
byproducts: HF, CO2; dropping of water under ice cooling;
参考文献
Ragulin, L. N.; Ropalo, P. P.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1685 - 1688
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1754 - 1758
C.A., 1968 , vol. 68, p. 48977
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Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
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Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
hydrogen fluoride T=60°C; 72 h;
参考文献
Banks,R.E. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1171 - 1179
反应条件
in formamide Irradiation (UV/VIS); 35°C , 20 h , irradiation of volatile product in presence of bromine;
参考文献
Banks,R.E. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1171 - 1179
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Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
参考文献
Eleev,A.F. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1974 , vol. 23, p. 363 - 366
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , vol. 23, p. 397 - 400
反应条件
intermediate decomp. in presence of anion-stabilizing agent;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
hydrogen fluoride; copper; fluorine T=130 - 140°C; Title compound not separated from byproducts.;
参考文献
Nurgalieva; Bispen; Il'in; Moldavskii; Rozhkova
Russian Journal of Applied Chemistry, 2007 , vol. 80, # 9 p. 1562 - 1565
参考文献
Ermolov, A. F.; Eleev, A. F.; Kutepov, A. P.; Sokol'skii, G. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1999 - 2000
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2239 - 2240