2-((4-溴苯基)(甲基)氨基)乙腈合成路线 （共 14 条）
反应条件
ruthenium trichloride; oxygen; acetic acid in methanol T=60°C; P=760 Torr; 2 h;
参考文献
Murahashi, Shun-Ichi; Komiya, Naruyoshi; Terai, Hiroyuki; Nakae, Takahiro
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15312 - 15313
反应条件
C47H45Cl2N5Ru2(2+)*2F6P(1-); dihydrogen peroxide; acetic acid in methanol T=60°C; 10 h; Inert atmosphere;
参考文献
Lo, Ying-Hao; Liu, Yi-Hung; Peng, Shie-Ming; Liu, Shiuh-Tzung
Journal of the Chinese Chemical Society, 2013 , vol. 60, # 7 p. 839 - 845
反应条件
tert.-butylhydroperoxide; [AubpyCl2]Cl in methanol; decane T=20°C; 5 h; regioselective reaction;
参考文献
Zhang, Yan; Peng, Hao; Zhang, Ming; Cheng, Yixiang; Zhu, Chengjian
Chemical Communications, 2011 , vol. 47, # 8 p. 2354 - 2356
反应条件
ruthenium trichloride; dihydrogen peroxide in methanol; water T=50°C; 3 h;
参考文献
Verma, Sanny; Jain, Suman L.; Sain, Bir
Catalysis Letters, 2011 , vol. 141, # 6 p. 882 - 885
反应条件
in formic acid 3 h; Heating / reflux;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/40110 A1, 2005 ;
Location in patent: Page/Page column 103 ;
反应条件
tetra-(n-butyl)ammonium iodide in water; tert-butyl alcohol T=60°C; 36 h;
参考文献
Zhang, Chao; Liu, Chunmei; Shao, Ying; Bao, Xiaoguang; Wan, Xiaobing
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17917 - 17925
反应条件
chloroform; bromine man faellt mit Aether und behandelt das Reaktionsprodukt mit Wasser;
参考文献
Liang, Yah-Long; Fang, Jim-Min; Chow, Tahsin; Ho, Tong-Ing; Lee, Chi-Rung; Wang, Yu
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5742 - 5747
反应条件
in 1,2-dichloro-ethane 1 h; Heating;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Krasutsky, Alexei P.; Bolz, Jason T.; Mismash, Brian; et al.
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7975 - 7978
反应条件
1: <10 3: chloroform; bromine / man faellt mit Aether und behandelt das Reaktionsprodukt mit Wasser View Scheme
参考文献
v. Braun
Chemische Berichte, 1908 , vol. 41, p. 2117
Chemische Berichte, 1909 , vol. 42, p. 2056
参考文献
v.Braun
Chemische Berichte, 1908 , vol. 41, p. 2103
