N,N-双(三甲基硅基)甲酰胺合成路线 （共 18 条）
反应条件
triethylamine in benzene 1 h; Heating;
参考文献
Johnson, A. Peter; Luke, Richard W. A.; Steele, Robert W.; Boa, Andrew N.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 9 p. 883 - 893
参考文献
Klinge, Michael; Cheng, Hengmiao; Zabriskie, T. Mark; Vederas, John C.
Journal of the Chemical Society, Chemical Communications, 1994 , # 11 p. 1379 - 1380
反应条件
1) THF, -78 deg C, 30 min, 2a) -78 deg C, 30 min, 2b) -78 to 0 deg C, 2 h, 2c) RT, 16 h; Yield given. Multistep reaction;
参考文献
Shih
Tetrahedron Letters, 1993 , vol. 34, # 4 p. 595 - 598
反应条件
1) THF, -78 deg C, 30 min, 2a) -78 deg C, 30 min, 2b) -78 to 0 deg C, 2 h, 2c) RT, 16h; Yield given. Multistep reaction;
参考文献
Shih
Tetrahedron Letters, 1993 , vol. 34, # 4 p. 595 - 598
反应条件
T=100°C; 0.0666667 h;
参考文献
Lazukina, L. A.; Mushkalo, I. L.; Neplyuev, V. M.; Kukhar', V. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2114 - 2117
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2417 - 2420
参考文献
Kantlehner,W. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 512 - 527
反应条件
- 78 - 0 deg C; Yield given. Yields of byproduct given;
参考文献
Uyehara; Suzuki; Yamamoto
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4275 - 4278
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 1 h, 2.) THF, -70 deg C, 1 h, room temp., 2 h; Yield given. Multistep reaction;
参考文献
Uyehara; Suzuki; Yamamoto
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4275 - 4278
反应条件
- 78 - 0 deg C; Yield given. Yields of byproduct given;
参考文献
Uyehara; Suzuki; Yamamoto
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4275 - 4278
反应条件
lithium diisopropyl amide
1.) THF, -78 deg C, 1 h, 2.) THF, -70 deg C, 1 h, room temp., 2 h; Yield given. Multistep reaction;
参考文献
Uyehara; Suzuki; Yamamoto
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4275 - 4278
