2-三甲基硅基-1,3-二噻吩合成路线 （共 37 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane 0.5 h; Ambient temperature;
参考文献
Porskamp, P. A. T. W.; Leij, M. van der; Lammerink, B. H. M.; Zwanenburg, B.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 9 p. 400 - 404
反应条件
in tetrahydrofuran; hexane -78 deg C to room t.;
参考文献
Page, Philip C. Bulman; van Niel, Monique B.; Westwood, Donald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 269 - 276
反应条件
n-butyllithium 1.) THF, -20 deg C, 2.5 h; 2.) THF, room temp., 10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Liebigs Annalen der Chemie, , # 5 p. 944 - 949
反应条件
1: 2-(trimethylsilyl)-1,3-dithiane With n-butyllithium in tetrahydrofuran; hexanes T=-78 - 0°C; 1 h; 2: 5-hydroxypentan-2-one in tetrahydrofuran; hexanes T=20°C;
参考文献
Xu, Hai-Chao; Moeller, Kevin D.
Journal of the American Chemical Society, 2010 , vol. 132, # 8 p. 2839 - 2844
反应条件
in tetrahydrofuran; dichloromethane; water
参考文献
Hatanaka,Minoru; KANEGAFUCHI KAGAKU KOGYO KABUSHIKI KAISHA
Patent: EP260092 A2, 1988 ;
反应条件
n-butyllithium Multistep reaction;
参考文献
Hatanaka, Minoru
Tetrahedron Letters, 1987 , vol. 28, # 1 p. 83 - 86
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-10°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Andarsen, Niels H.; McCrae, David A.; Grotjahn, Douglas B.; Gabhe, Satish Y.; Theodore, Louis J.; et al.
Tetrahedron, 1981 , vol. 37, # 23 p. 4069 - 4079
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-10°C; 0.333333 h; Title compound not separated from byproducts;
参考文献
Andarsen, Niels H.; McCrae, David A.; Grotjahn, Douglas B.; Gabhe, Satish Y.; Theodore, Louis J.; et al.
Tetrahedron, 1981 , vol. 37, # 23 p. 4069 - 4079
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Andarsen, Niels H.; McCrae, David A.; Grotjahn, Douglas B.; Gabhe, Satish Y.; Theodore, Louis J.; et al.
Tetrahedron, 1981 , vol. 37, # 23 p. 4069 - 4079
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-60°C; 1 h; Title compound not separated from byproducts;
参考文献
Andarsen, Niels H.; McCrae, David A.; Grotjahn, Douglas B.; Gabhe, Satish Y.; Theodore, Louis J.; et al.
Tetrahedron, 1981 , vol. 37, # 23 p. 4069 - 4079
