1: With PyBH2I in dichloromethane T=20°C; 2: With sodium hydroxide; dihydrogen peroxide in methanol; dichloromethane T=0 - 20°C; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 127, # 16 p. 5766 - 5767
potassium hydroxide; hydrogen; platinum on activated charcoal in 2,2,4-trimethylpentane; water T=50°C; P=760 Torr; 6 h; other reagent, reaction time, various KOH concentrations, pH effect; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3934 - 3939