1: 85 percent / ZnI2 / 3 h / 25 °C
2: LiN(iPr)2 / tetrahydrofuran; hexane / 2 h / -78 °C
3: tetrahydrofuran / -78 °C / var. solvents; var. bases; var. complex reagents; var. temp.; var. subst. 1-cyano-1-O-substituted allyl lithium compounds
View Scheme
参考文献
Huenig, Siegfried; Reichelt, Helmut
Chemische Berichte, 1986 , vol. 119, # 6 p. 1772 - 1800
1: LiN(iPr)2 / tetrahydrofuran; hexane / 2 h / -78 °C
2: tetrahydrofuran / -78 °C / var. solvents; var. bases; var. complex reagents; var. temp.; var. subst. 1-cyano-1-O-substituted allyl lithium compounds
View Scheme
参考文献
Huenig, Siegfried; Reichelt, Helmut
Chemische Berichte, 1986 , vol. 119, # 6 p. 1772 - 1800
lithium diisopropyl amide in tetrahydrofuran
1) -78 deg C, 2) to r.t., overnight; Yield given. Yields of byproduct given. Title compound not separated from byproducts;