5,6,7,8-四氢喹啉合成路线 （共 92 条）
反应条件
hydrogen; acetic acid; Pearlman's catalist in tetrahydrofuran; ethanol T=20 - 60°C; 23.5 h;
参考文献
RENOVIS, INC.; DUNCTON, Matthew; O'MAHONY, Donogh, John, Roger; COX, Matthew
Patent: WO2010/59610 A1, 2010 ;
Location in patent: Page/Page column 63 ;
WO 2010/059610 A1
反应条件
5 Ru/MgO; hydrogen in tetrahydrofuran T=150°C; P=38002.6 Torr; 0.7 h; TimeConcentrationPressure;
参考文献
Journal of Catalysis, , vol. 311, p. 357 - 368
反应条件
hydroxylamine hydrochloride in ethanol T=80°C; 3 h;
参考文献
Pham, Van Cuong; Jossang, Akino; Chiaroni, Angele; Sevenet, Thierry; Bodo, Bernard
Tetrahedron Letters, 2002 , vol. 43, # 42 p. 7565 - 7568
反应条件
hydrogen; nickel T=210°C; P=7600 Torr; or Ru/C, 100 atm, 150 deg C, and competitive hydrogenation with isoquinoline; Rate constant;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 11 p. 3167 - 3174
反应条件
aluminium trichloride; cyclohexane T=90°C; 15 h;
参考文献
Koltunov, Konstantin Yu.; Prakash, G. K. Surya; Rasul, Golam; Olah, George A.
Journal of Organic Chemistry, 2002 , vol. 67, # 12 p. 4330 - 4336
反应条件
aluminium trichloride; cyclohexane T=90°C; 90 h;
参考文献
Koltunov, Konstantin Yu.; Prakash, G. K. Surya; Rasul, Golam; Olah, George A.
Journal of Organic Chemistry, 2002 , vol. 67, # 12 p. 4330 - 4336
反应条件
hydrogen; 10percent Pd/C in trifluoroacetic acid
参考文献
Zhu, Man; Qiu, Zhilei; Hiel, Gary P.; Sieburth, Scott McN.
Journal of Organic Chemistry, 2002 , vol. 67, # 10 p. 3487 - 3493
反应条件
molybdenum disulfide; hydrogen in decane T=340°C; P=22502.3 Torr; Kinetics; Reagent/catalyst;
参考文献
Applied Catalysis A: General, , vol. 469, p. 173 - 182
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; Further byproducts given;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
dimethyl-disulfide; hydrogen; Ir sulfide in various solvent(s) T=349.9°C; P=37503 Torr; 3 h; Further byproducts given;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 11-12 p. 885 - 890
