反应条件
1: cyclohexane / 8 h / 70 - 80 °C / Large scale reaction 2: triethylamine / dichloromethane / 5 - 35 °C / Large scale reaction 3: hydrogenchloride / water / 98 - 102 °C / Large scale reaction 4: chlorosulfonic acid / dichloromethane / 0 °C / Reflux 5: water / tetrahydrofuran / 24 h / Reflux View Scheme
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649