1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78 - -40°C; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) Substitution; 4 h; Heating;
参考文献
Anderson, Benjamin A.; Bell, Edward C.; Ginah, Francis O.; Harn, Nancy K.; Pagh, Lisa M.; Wepsiec, James P.
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8224 - 8228