disodium hydrogenphosphate; sodium amalgam in tetrahydrofuran; methanol
14 h;
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: phosphorus pentasulfide
2: tetrahydrofuran / 1 h / 0 °C
3: Et3N / CH2Cl2 / 72 h / 20 °C
4: 86 percent / sodium amalgam; Na2HPO4 / tetrahydrofuran; methanol / 14 h
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: tetrahydrofuran / 1 h / 0 °C
2: Et3N / CH2Cl2 / 72 h / 20 °C
3: 86 percent / sodium amalgam; Na2HPO4 / tetrahydrofuran; methanol / 14 h
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
