反应条件
in tetrahydrofuran; hexane; toluene
(strict exclusion of air and moisture), Fe complex in THF cooled to -20°C, treated dropwise wit 2 equiv. of Et2AlCl in hexane, stirred atroom temp. for 20 h, evapd.(vac.), dissolved (toluene), treated with py ridine, stirred for 20 h; centrifuged, evapd.(vac.), washed (hexane), dried (vac.), dissolved (Et2O), filtered, evapd.(vac.), elem. anal.;
参考文献
Wrackmeyer, Bernd; Klimkina, Elena V.; Milius, Wolfgang
European Journal of Inorganic Chemistry, 2009 , # 21 p. 3155 - 3162
