1-(2-羟基-5-甲基苯基)-1-丙酮合成路线 （共 31 条）
反应条件
aluminium trichloride 1.) 70 -> 80 deg C, 2 h, 2.) 120 deg C, 40 min;
参考文献
Burdeska, K.
Synthesis, 1982 , # 11 p. 940 - 942
反应条件
boron trifluoride diethyl etherate 0.0416667 h; microwave irradiation;
参考文献
Naeimi; Moradi
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 12 p. 1757 - 1759
反应条件
C5H2Ph4; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper diacetate in 1,2-dichloro-ethane T=120°C; P=3750.38 Torr; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Shi, Zhuangzhi; Schroeder, Nils; Glorius, Frank
Angewandte Chemie - International Edition, 2012 , vol. 51, # 32 p. 8092 - 8096
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=110 - 120°C; 8 h;
参考文献
Krzyzanowska, Ewa; Olszanowski, A.; Juskowiak, M.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 4 p. 617 - 630
反应条件
aluminium trichloride in dichloromethane
参考文献
Dijkstra, P. J.; Steen, B. J. van; Hams, B. H. M.; Hertog, H. J. den; Reinhoudt, D. N.
Tetrahedron Letters, 1986 , vol. 27, # 27 p. 3183 - 3186
反应条件
1.1: NaOH / acetonitrile / 1.25 h 1.2: acetonitrile / 16 h / 20 °C 2.1: AlCl3 / 1.5 h / 110 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 11 p. 3488 - 3495
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chemische Berichte, , vol. 47, p. 3314
Chemische Berichte, , vol. 50, p. 1604
Journal of the American Chemical Society, , vol. 37, p. 1845
反应条件
aluminium trichloride T=180°C; 1 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 7 p. 539 - 548
反应条件
aluminium trichloride in neat (no solvent) T=150°C; 1 h; MechanismProduct distribution;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 7 p. 539 - 548
反应条件
aluminium trichloride T=170°C;
参考文献
Doklady Akademii Nauk SSSR, , vol. 109, p. 319
Doklady Chemistry, 106-111 <1956> 389
