2,2'-硫代二乙酸二乙酯合成路线 （共 25 条）
反应条件
sodium sulfide; sodium hydroxide; sodium dihydrogenphosphate; tri-n-butylmethylammonium chloride in water; toluene T=30 - 35°C; pH=6.0; 5 h;
参考文献
SALTIGO GMBH
Patent: US2009/163736 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
sulfuric acid Heating / reflux;
参考文献
E. I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2006/73968 A2, 2006 ;
Location in patent: Page/Page column 21-22 ;
反应条件
phenylmethanethiol; copper(l) chloride
参考文献
Journal of Organic Chemistry, , vol. 33, # 2 p. 544 - 547
反应条件
sodium sulfide in ethanol
参考文献
Journal of Organic Chemistry, , vol. 33, p. 563 - 568
反应条件
(i) Na, Et2O, (ii) /BRN= 506455/; Multistep reaction;
参考文献
Helvetica Chimica Acta, , vol. 47, p. 1748 - 1753
反应条件
potassium carbonate in chloroform
参考文献
Journal of Organic Chemistry, , vol. 75, # 2 p. 472 - 475
反应条件
[BnEt3N]2MoS4 in chloroform 6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 22, # 22 p. 3277 - 3284
反应条件
1: Me2S / dimethylsulfoxide View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 955 - 961
反应条件
[BnEt3N]2MoS4 in solid 0.166667 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 6 p. 767 - 768
反应条件
sulfuric acid Veresterung;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 59, p. 423,432
