二异丙基磷光体amidous二氯化物合成路线 （共 26 条）
反应条件
phosphorus trichoride in hexane T=0 - 40°C;
参考文献
Drent, Eite; Van Dijk, Rudmer; Van Ginkel, Roel; Van Oort, Bart; Pugh, Robert I.
Chemical Communications, 2002 , # 9 p. 964 - 965
参考文献
Chemische Berichte, , vol. 123, # 6 p. 1245 - 1251
反应条件
1: 3-hydroxy-propionitrile With N-ethyl-N,N-diisopropylamine; 1-n-butyl-2,3-dimethylimidazolium bistrifluoromethylsulfonylamide; phosphorus trichoride 2: diisopropylamine 0.666667 h; chemoselective reaction;
参考文献
Green Chemistry, , vol. 11, # 9 p. 1391 - 1396
反应条件
1: 3-hydroxy-propionitrile With N-ethyl-N,N-diisopropylamine; 1-n-butyl-2,3-dimethylimidazolium bistrifluoromethylsulfonylamide; phosphorus trichoride 2: diisopropylamine 0.666667 h; chemoselective reaction;
参考文献
Green Chemistry, , vol. 11, # 9 p. 1391 - 1396
反应条件
hydrogenchloride Ambient temperature; Product distribution;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 18, p. 125 - 128
反应条件
triethylamine in diethyl ether T=20°C; 3 h;
参考文献
Chen, Shui-Bing; Li, Yan-Mei; Luo, Shi-Zhong; Zhao, Gang; Tan, Bo; Zhao, Yu-Fen
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 277 - 291
反应条件
ozone in dichloromethane T=0°C;
参考文献
Caminade, Anne-Marie; El Khatib, Fayez; Baceiredo, Antoine; Koenig, Max
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 365 - 368
反应条件
1: 60 percent / tetrahydrofuran / -78 °C 2: HCl / diethyl ether / -10 °C View Scheme
参考文献
van Assema, Sander G.A.; Kraikivskii, Petr B.; Zelinskii, Stanislav N.; Saraev, Vitaly V.; de Jong, G. Bas; de Kanter, Frans J.J.; Schakel, Marius; Chris Slootweg; Lammertsma, Koop
Journal of Organometallic Chemistry, 2007 , vol. 692, # 11 p. 2314 - 2323
反应条件
N-ethyl-N-isopropylamine 1.) CH2Cl2, -10 grad C, 30 min, 2.) CH2Cl2, 30 min; Yield given. Multistep reaction;
参考文献
Tanaka, Toshiki; Tamatsukuri, Sigeru; Ikehara, Morio
Tetrahedron Letters, 1986 , vol. 27, # 2 p. 199 - 202
反应条件
triethylamine in tetrahydrofuran T=-20 - 20°C; Condensation;
参考文献
Scheigetz, John; Roy, Bruno
Synthetic Communications, 2000 , vol. 30, # 8 p. 1437 - 1445
