反应条件
in diethyl ether
dropwise addn. (stirring) of a soln. of P(NEt2)3 in anhydrous ether to a soln. of C6F5Br and the germyl halide in pentane (under Ar), stirred (20°C, 1 h); filtered, solvent distd. off (vac. evaporator), residue filtered off, distd. (vac.);
参考文献
Bardin, V. V.; Aparina, L. N.; Pressman, L. S.; Furin, G. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 2 p. 1983
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 9, p. 2153 - 2154
