1,1'-[乙亚基二(氧基)]二丁烷合成路线 （共 77 条）
反应条件
hydrogenchloride in acetone
T=54°C; 5 h;
参考文献
Voronkov, M. G.; Keiko, N. A.; Kuznetsova, T. A.; Frolov, Yu. L.; Kalikhman, I. D.; Chuvashev, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1738 - 1741
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2043 - 2047
反应条件
hydrogenchloride in diethyl ether
3 - 11 h; Reflux;
参考文献
Lobanova; Stankevich; Kukharev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1289 - 1296
Zh. Org. Khim., 2012 , vol. 48, # 10 p. 1295 - 1301,7
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide
参考文献
Croxall; Glavis; Neher
Journal of the American Chemical Society, 1948 , vol. 70, p. 2806
Full Text Show Details
Roehm and Haas
Patent: US2446171 , 1945 ;
反应条件
hydrogenchloride in acetone
T=54°C; 5 h;
参考文献
Voronkov, M. G.; Keiko, N. A.; Kuznetsova, T. A.; Frolov, Yu. L.; Kalikhman, I. D.; Chuvashev, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1738 - 1741
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2043 - 2047
反应条件
hydrogenchloride in acetone
T=54°C; 5 h;
参考文献
Voronkov, M. G.; Keiko, N. A.; Kuznetsova, T. A.; Frolov, Yu. L.; Kalikhman, I. D.; Chuvashev, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1738 - 1741
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2043 - 2047
反应条件
hydrogenchloride in diethyl ether
3 - 11 h; Reflux;
参考文献
Lobanova; Stankevich; Kukharev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 10 p. 1289 - 1296
Zh. Org. Khim., 2012 , vol. 48, # 10 p. 1295 - 1301,7
反应条件
tert-butyl peroxy pivalate in acetonitrile
T=68°C; Further byproducts given;
参考文献
Boutevin, B.; Cersosimo, F.; Youssef, B.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 403 - 418
反应条件
C3F7COOH
T=50 - 55°C; 2 h;
参考文献
Papsheva, N. P.; Gerasimova, V. V.; Nedolya, N. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 10 p. 2011 - 2012
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 10 p. 2230 - 2232
反应条件
boron trifluoride-methanol; mercury(II) oxide
参考文献
Hinton; Nieuwland
Journal of the American Chemical Society, 1930 , vol. 52, p. 2892,2893
反应条件
hydrogenchloride; bromo-phenylcarboxamide in acetone
T=54°C; 5 h; Yields of byproduct given;
参考文献
Voronkov, M. G.; Keiko, N. A.; Kuznetsova, T. A.; Frolov, Yu. L.; Kalikhman, I. D.; Chuvashev, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1738 - 1741
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2043 - 2047
