氯(二异丙基氨基)甲氧基膦合成路线 (共 8 条)
反应条件
tris(2,4,6-tribromo-phenoxy)dichlorophosphorane in pyridine Title compound not separated from byproducts;
参考文献
Wada; Ishikawa; Hata
Tetrahedron Letters, 1990 , vol. 31, # 44 p. 6363 - 6366
参考文献
McBride, L. J.; Caruthers, M. H.
Tetrahedron Letters, 1983 , vol. 24, # 3 p. 245 - 248
反应条件
in tetrahydrofuran T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 48, # 35 p. 6080 - 6083
反应条件
in chloroform-d1 Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1045 - 1048
反应条件
1: 88 percent / tetrahydrofuran / -35 - 20 °C 2: CHCl3 / Ambient temperature View Scheme
参考文献
Dias; Mornet; Kotoujansky
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 1 p. 73 - 78
反应条件
in tetrahydrofuran T=-35 - 20°C;
参考文献
Dias; Mornet; Kotoujansky
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 1 p. 73 - 78
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran
Ambient temperature;
参考文献
Adams, Steven P.; Kavka, Kamila S.; Wykes, Evan J.; Holder, Sarah B.; Galluppi, Gerald R.
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 661 - 663
参考文献
Herdering, Wilhelm; Seela, Frank
Journal of Organic Chemistry, 1985 , vol. 50, # 25 p. 5314 - 5323