2-羟亚氨基-2-苯乙腈合成路线 （共 43 条）
反应条件
potassium hydroxide; nitrogen(II) oxide in methanol T=60°C; P=1875.19 Torr; 24 h; Inert atmosphere;
参考文献
Scott Bohle; Perepichka, Inna
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1621 - 1626
反应条件
sodium hydroxide in ethanol
参考文献
Dow AgroSciences LLC
Patent: US6413997 B1, 2002 ;
反应条件
nitrogen(II) oxide in methanol T=0 - 3°C; P=1875.19 Torr; 48 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 4 p. 1621 - 1626
反应条件
sulfuric acid in dichloromethane; ethyl acetate T=20°C; 0.0833333 h;
参考文献
Zelenov; Voronin; Churakov; Klenov; Strelenko, Yu. A.; Tartakovsky
Russian Chemical Bulletin, 2012 , vol. 61, # 2 p. 351 - 354
Izv. Akad. Nauk, Ser. Khim., 2012 , # 2 p. 349 - 352,4
反应条件
nitrogen(II) oxide in methanol T=-20°C; P=1875.19 Torr; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 4 p. 1621 - 1626
反应条件
triethylamine in water; 1,2-dichloro-ethane; isopropyl alcohol T=-5 - 20°C; Substitution; 4 h;
参考文献
Synthetic Communications, , vol. 29, # 22 p. 3863 - 3868
反应条件
sulfuric acid T=20°C; 0.166667 h;
参考文献
Zelenov; Voronin; Churakov; Klenov; Strelenko, Yu. A.; Tartakovsky
Russian Chemical Bulletin, 2012 , vol. 61, # 2 p. 351 - 354
Izv. Akad. Nauk, Ser. Khim., 2012 , # 2 p. 349 - 352,4
反应条件
1: tert-butyl hypochlorite / 1,2-dichloro-ethane; propan-2-ol / 30 h / -12 - -10 °C 2: Et3N / 1,2-dichloro-ethane; propan-2-ol; H2O / 4 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 30, # 9 p. 1563 - 1567
反应条件
sodium hydroxide; ethanol; hydroxylamine hydrochloride; phenylglyoxime T=50 - 60°C;
参考文献
Chemische Berichte, , vol. 24, p. 3502
反应条件
ethanol; sodium ethanolate
参考文献
Journal of Organic Chemistry, , vol. 2, p. 183,191
