7,7-二氯二环[4.1.0]庚烷合成路线 (共 52 条)
反应条件
Fe(5,10,15,20-tetraphenylporphyrinate)CCl2 in benzene T=25°C; Irradiationother metalloporphyrin carbene and vinylidnene complexes, other alkenes; other solvents; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 118, # 22 p. 5306 - 5307
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 1.) 8 h, reflux, 2.) 12 h, room temperature;
参考文献
Hashem, Md. Abul
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 424 - 429
反应条件
in cyclohexane T=21°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 112, # 8 p. 3217 - 3218
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 18, # 16-17 p. 2117 - 2122
反应条件
potassium fluoride; tetra-(n-butyl)ammonium iodide in dichloromethane T=40°C; 40 h;
参考文献
Dehmlow, Eckehard V.; Leffers, Willi
Journal of Organometallic Chemistry, 1985 , vol. 288, p. C41 - C43
参考文献
Journal of the American Chemical Society, , vol. 127, # 41 p. 14206 - 14207
反应条件
in pentane T=10.09°C; Kinetics; Further Variations:Temperatures;
参考文献
Journal of the American Chemical Society, , vol. 130, # 17 p. 5634 - 5635
参考文献
Journal of Organic Chemistry, , vol. 24, p. 1733
反应条件
N-benzyl-N,N,N-triethylammonium chloride; tetra-n-butylammonium tetrafluoroborate; carbon in acetonitrile T=5 - 8°C; other solvents, other bases, other temperatures, other cathode; Product distributionMechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 8.1 p. 1633 - 1637
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1802 - 1806
反应条件
carbon T=-196.1°C; other chlorofluoromethanes and CCl4;
参考文献
Journal of the American Chemical Society, , vol. 116, # 20 p. 9405 - 9406