(3,3-二甲基-2-氧代丁基)膦酸二乙酯合成路线 （共 10 条）
反应条件
C-200 (barium hydroxide) in 1,4-dioxane; water T=70°C; 0.166667 h;
参考文献
Ibarra, Carlos Alvarez; Arias, Selma; Fernandez, Maria J.; Sinisterra, Jose V.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 503 - 508
反应条件
magnesium; trimethylphosphane; CoCl2 in tetrahydrofuran
T=20°C;
参考文献
Orsini, Fulvia; Di Teodoro, Emanuela; Ferrari, Marinella
Synthesis, 2002 , # 12 p. 1683 - 1688
反应条件
n-butyllithium; lithium diisopropyl amide in tetrahydrofuran; hexane
T=-60°C;
参考文献
Aboujaoude, Elie Elia; Collignon, Noel; Teulade, Marie-Paule; Savignac, Philippe
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 25, p. 57 - 62
反应条件
[{RuCl((S)-MeO-BIPHEP)}2(μ-Cl)3][NH2Me2]; hydrogen in methanol
T=50°C; P=7500.75 Torr; 24 h; Autoclave; enantioselective reaction;
参考文献
Prevost, Sebastien; Gauthier, Sebastien; De Andrade, Maria Cristina Cano; Mordant, Celine; Touati, Ali Rhida; Lesot, Philippe; Savignac, Philippe; Ayad, Tahar; Phansavath, Phannarath; Ratovelomanana-Vidal, Virginie; Genet, Jean-Pierre
Tetrahedron Asymmetry, 2010 , vol. 21, # 11-12 p. 1436 - 1446
参考文献
Sturtz,G.
Bulletin de la Societe Chimique de France, 1964 , p. 2349 - 2357
反应条件
tin(ll) chloride in dichloromethane
4 h; Ambient temperature; Yield given;
参考文献
Holmquist, Christopher R.; Roskamp, Eric J.
Tetrahedron Letters, 1992 , vol. 33, # 9 p. 1131 - 1134
反应条件
tert.-butyl lithium; lithium hexamethyldisilazane
Yield given. Multistep reaction;
参考文献
Sampson, Paul; Hammond, Gerald B.; Wiemer, David F.
Journal of Organic Chemistry, 1986 , vol. 51, # 23 p. 4342 - 4347
反应条件
Yield given. Multistep reaction;
参考文献
Lee, Koo; Wiemer, David F.
Journal of Organic Chemistry, 1991 , vol. 56, # 19 p. 5556 - 5560
反应条件
(i) nBuLi, hexane, THF, (ii) Cu2I2, (iii) /BRN= 385668/, Et2O; Multistep reaction;
参考文献
Mathey,F.; Savignac,P.
Tetrahedron, 1978 , vol. 34, p. 649 - 654
参考文献
Zygmunt,J. et al.
Synthesis, 1978 , p. 609 - 612
