4-甲基-N-(2-甲基苯基)苯磺酰胺合成路线 (共 22 条)
参考文献
Alp, Cemalettin; Oezsoy, Seyda; Alp, Nurdan Alcan; Erdem, Deryanur; Gueltekin, Mehmet Serdar; Kuefrevioglu, Oemer Irfan; Sentuerk, Murat; Supuran, Claudiu T.
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 6 p. 818 - 824
反应条件
potassium carbonate in water 7 h; Reflux;
参考文献
Azarifar, Davood; Soleimanei, Fatemeh
RSC Advances, 2014 , vol. 4, # 24 p. 12119 - 12126
反应条件
1,10-phenanthroline; palladium (II) trifluoroacetate; oxygen in toluene T=140°C; 40 h;
参考文献
Cao, Xiangxiang; Bai, Yang; Xie, Yanjun; Deng, Guo-Jun
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 383-384, p. 94 - 100
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in N,N-dimethyl-formamide T=100°C; 24 h;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in 1,1-dimethylpropan-1-ol T=80°C; 15 h; Inert atmosphere;
参考文献
Shekhar, Shashank; Dunn, Travis B.; Kotecki, Brian J.; Montavon, Donna K.; Cullen, Steven C.
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4552 - 4563
反应条件
CyGemPhos; water; palladium diacetate; caesium carbonate in 1,4-dioxane T=150°C; Buchwald-Hartwig coupling; 24 h;
参考文献
Falk, Florian C.; Froehlich, Roland; Paradies, Jan
Chemical Communications, 2011 , vol. 47, # 39 p. 11095 - 11097
反应条件
copper(l) iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=100 - 110°C; 13 h; Inert atmosphere;
参考文献
Hosseinzadeh, Rahman; Tajbakhsh, Mahmood; Mohadjerani, Maryam; Alikarami, Mohammad
Journal of Chemical Sciences, 2010 , vol. 122, # 2 p. 143 - 148
反应条件
FeCl3·6H2O T=60°C; 4 h; Inert atmosphere;
参考文献
Organic Preparations and Procedures International, , vol. 45, # 1 p. 28 - 43
反应条件
[(tris(3,5-dimethylpyrazol-1-yl)methane)Fe(NCMe)3](BF4)2 in dichloromethane T=19.84°C; Overall yield = 60 percent; regioselective reaction;
参考文献
Organometallics, , vol. 31, # 23 p. 8055 - 8058
反应条件
1: cyanic acid sodium salt / water / 0.17 h / |Reflux 2: potassium carbonate / water / 7 h / |Reflux View Scheme
参考文献
RSC Advances, , vol. 4, # 24 p. 12119 - 12126